Publications related to Observation of 1H-1H J-couplings in fast magic-angle-spinning solid-state NMR spectroscopy

Related publications (7)

Structure determination by NMR Crystallography, from microcrystalline powders to amorphous molecular solids

Structure elucidation of amorphous materials and microcrystalline solids is one of the key challenges in chemistry today. While techniques such as single crystal diffraction and cryo-electron microscopy are generally not able to characterize such materials ...

AIP Publishing2025

B(0)shimming for in vivo magnetic resonance spectroscopy: Experts' consensus recommendations

Rolf Gruetter, Cristina Ramona Cudalbu Moldovan

Magnetic resonance spectroscopy (MRS) and spectroscopic imaging (MRSI) allow the chemical analysis of physiological processes in vivo and provide powerful tools in the life sciences and for clinical diagnostics. Excellent homogeneity of the static B(0)magn ...

2020

Hyperpolarization transfer pathways in inorganic materials

David Lyndon Emsley, Brennan James Walder, Pinelopi Moutzouri, Snaedis Björgvinsdóttir

Dynamic nuclear polarization can be used to hyperpolarize the bulk of proton-free inorganic materials in magic angle spinning NMR experiments. The hyperpolarization is generated on the surface of the material with incipient wetness impregnation and from th ...

Academic Press Inc - Elsevier Science2020

Homonuclear ADAPT: A general preparation route to long-lived nuclear singlet order

Gabriele Stevanato

We introduce a simple strategy to access and readout nuclear singlet order based on the alternate repetition of hard pulses and delays. We demonstrate the general applicability of the method by accessing nuclear singlet order in spin systems characterized ...

Academic Press Inc - Elsevier Science2019

Single crystals of superconducting SmFeAsOHx: Structure and properties

László Forró, Alla Arakcheeva, Richard Gaal, Sergiy Katrych, Andrea Pisoni, Ping Huang, Péter Krisztián Matus

We report the synthesis, structure, and superconducting properties of single crystals of SmFeAsOHx. The crystals were grown at high pressure and high temperature using a cubic anvil technique. H-1-NMR studies confirm the presence of H atoms in the samples. ...

Amer Physical Soc2016

Development of Ultraviolet Photon Echo Experiments for the Study of Molecular Dynamics in Solution

Ahmad Ajdar Zadeh Oskouei

This thesis work concerns the development and applications of ultrafast optical techniques and in particular photon echo in the UV range (< 300 nm). Development of these techniques in the UV range is important for studying molecular dynamics in solution, s ...

EPFL2011

The Torsional Barriers of 2-Hydroxy- and 2-Fluorobiphenyl: Small but Measurable

By making use of a novel diastereotopicity probe, namely C(CF3)(2)OH, it has been possible to measure by very low temperature F-19 NMR spectroscopy the elusive aryl aryl rotation barriers of biphenyls bearing an OH or F group in one rill position. The expe ...

2010