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New schemes are introduced that allow one to improve the resolution in the indirect dimension of single-scan 'ultrafast' two-dimensional NMR spectra. The methods combine undersampling with band-selective pulses to recover signals that lie outside the detection bandwidth. The efficiency is illustrated for homonuclear total correlation spectroscopy (TOCSY) of quinidine. (C) 2008 Elsevier Inc. All rights reserved.
David Lyndon Emsley, Pierrick Berruyer, Saumya Badoni
Raffaella Buonsanti, Anna Loiudice, Jan Vávra, Petru Pasquale Albertini