Structure determination by NMR Crystallography, from microcrystalline powders to amorphous molecular solids

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While 1H-1H J-couplings are the cornerstone of all spectral assignment methods in solution-state NMR, they are yet to be observed in solids. Here we observe 1H-1H J-couplings in plastic crystals of (1S)-(−)-camphor in solid-state NMR at magic angle spinnin ...

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A detailed investigation of Ba2MnGe2O7 was performed in its low-temperature magnetoelectric state combining neutron diffraction with magnetization measurements on single crystals. In the paramagnetic state at 10 K, polarized neutron diffraction was applied ...

In the FeGP cofactor of [Fe]-hydrogenase, low-spin Fe-II is in complex with two CO ligands and a pyridinol derivative; the latter ligates the iron with a 6-acylmethyl substituent and the pyridinol nitrogen. A guanylylpyridinol derivative, 6-carboxymethyl-3 ...

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The photovoltaic perovskite, methylammonium lead triiodide [CH3NH3PbI3 (MAPbI(3))], is one of the most efficient materials for solar energy conversion. Various kinds of chemical and physical modifications have been applied to MAPbI(3) towards better unders ...

Organic-inorganic metal halide perovskites (MHPs) have recently attracted increasing attention as highly-efficient light-harvesting materials for photovoltaic applications. The technical ease of solution processing of these materials is one of their major ...

The synthesis of three potentially tetradentate, N2S2 Schiff-base-ligands, containing a disulfide bond, (LSSLThio)-S-Thio(L1), (LSSLBr)-S-Br(L2) and (LSSLDiMeO)-S-DiMeO (L3) are reported. These ligands undergo reductive disulfide bond scission upon reactio ...

We report the synthesis, structure, and superconducting properties of single crystals of SmFeAsOHx. The crystals were grown at high pressure and high temperature using a cubic anvil technique. H-1-NMR studies confirm the presence of H atoms in the samples. ...

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Structure determination by NMR Crystallography, from microcrystalline powders to amorphous molecular solids

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The influence of Cr concentration on the phase composition and properties of a unidirectionally crystallized ternary system Cr-Fe-Si before and after annealing

Observation of 1H-1H J-couplings in fast magic-angle-spinning solid-state NMR spectroscopy

Charge Dynamics Electron Microscopy Nanoscale Imaging of Femtosecond Plasma Dynamics

Magnetic structure of the magnetoelectric material Ba2MnGe2O7

In Vitro Biosynthesis of the [Fe]-Hydrogenase Cofactor Verifies the Proposed Biosynthetic Precursors

Ion-bridges and lipids drive aggregation of same-charge nanoparticles on lipid membranes

Magnetic excitations and structure of the topological semimetal YbMnSb2

Structural characterization and magnetic properties of chromium jarosite KCr3(OD)(6)(SO4)(2)

Molecular Engineering of Electrode Surfaces for Electrocatalysis

Highlights of the Science and Life of Peter Varga (1946-2018)

Halogen-bond driven self-assembly of perfluorocarbon monolayers on silicon nitride

Pressure-induced transformation of CH3NH3PbI3: the role of the noble-gas pressure transmitting media

Photo-physical Properties of Perovskites on Curved Surfaces

DNA-BSA interaction, cytotoxicity and molecular docking of mononuclear zinc complexes with reductively cleaved N2S2 Schiff base ligands

Single crystals of superconducting SmFeAsOHx: Structure and properties

In situ synthesis and simulation of polydisperse amphiphilic membranes