Publications related to Structure determination by NMR Crystallography, from microcrystalline powders to amorphous molecular solids

Related publications (16)

The influence of Cr concentration on the phase composition and properties of a unidirectionally crystallized ternary system Cr-Fe-Si before and after annealing

This paper describes the phase composition, morphological, chemical, and crystallographic prop- erties of silicide phases in Cr–Fe–Si alloy ingots obtained through directional solidification, both before and after annealing. The samples had a general formu ...

Pleiades Publishing Ltd2025

Observation of 1H-1H J-couplings in fast magic-angle-spinning solid-state NMR spectroscopy

David Lyndon Emsley, Daria Torodii, Jacob Brian Holmes

While 1H-1H J-couplings are the cornerstone of all spectral assignment methods in solution-state NMR, they are yet to be observed in solids. Here we observe 1H-1H J-couplings in plastic crystals of (1S)-(−)-camphor in solid-state NMR at magic angle spinnin ...

Nature Research2024

Charge Dynamics Electron Microscopy Nanoscale Imaging of Femtosecond Plasma Dynamics

Fabrizio Carbone, Tom Theodorus Antonius Lummen, Thomas La Grange, Ivan Madan, Giovanni Maria Vanacore, Gabriele Berruto, Simone Gargiulo, Francesco Barantani, Luca Piazza

Understanding and actively controlling the spatiotemporal dynamics of nonequilibrium electron clouds is fundamental for the design of light and electron sources, high power electronic devices, and plasma-based applications. However, electron clouds evolve ...

AMER CHEMICAL SOC2023

Magnetic structure of the magnetoelectric material Ba2MnGe2O7

Bálint Náfrádi

A detailed investigation of Ba2MnGe2O7 was performed in its low-temperature magnetoelectric state combining neutron diffraction with magnetization measurements on single crystals. In the paramagnetic state at 10 K, polarized neutron diffraction was applied ...

2023

In Vitro Biosynthesis of the [Fe]-Hydrogenase Cofactor Verifies the Proposed Biosynthetic Precursors

Xile Hu, Huijie Pan

In the FeGP cofactor of [Fe]-hydrogenase, low-spin Fe-II is in complex with two CO ligands and a pyridinol derivative; the latter ligates the iron with a 6-acylmethyl substituent and the pyridinol nitrogen. A guanylylpyridinol derivative, 6-carboxymethyl-3 ...

Wiley-VCH Verlag GmbH2022

Ion-bridges and lipids drive aggregation of same-charge nanoparticles on lipid membranes

Francesco Stellacci, Zekiye Pelin Güven

The control of the aggregation of biomedical nanoparticles (NP) in physiological conditions is crucial as clustering may change completely the way they interact with the biological environment. Here we show that Au nanoparticles, functionalized by an anion ...

ROYAL SOC CHEMISTRY2022

Magnetic excitations and structure of the topological semimetal YbMnSb2

Jian Rui Soh

INT UNION CRYSTALLOGRAPHY2021

Structural characterization and magnetic properties of chromium jarosite KCr3(OD)(6)(SO4)(2)

Sofie Janas

Potassium chromium jarosite, KCr3(OH)(6)(SO4)(2) (Cr-jarosite), is considered a promising candidate to display spin liquid behavior due to the strong magnetic frustration imposed by the crystal structure. However, the ground state magnetic properties have ...

ROYAL SOC CHEMISTRY2020

Molecular Engineering of Electrode Surfaces for Electrocatalysis

Patrick Eduard Alexa

Electrocatalysts play an important part on the route towards environmental friendly energy sources. They support modern technologies like fuel cells to move further away from the utilization of fossil fuels and the resulting CO2 emission into our atmospher ...

EPFL2020

Highlights of the Science and Life of Peter Varga (1946-2018)

Wolf-Dieter Schneider

Peter Varga has passed on October 27, 2018. His pioneering discoveries of chemical resolution at the atomic scale on surface alloys, atomic resolution of ultrathin alkali halides, nucleation of bcc iron in ultrathin films, and the microscopic structure of ...

2020

Halogen-bond driven self-assembly of perfluorocarbon monolayers on silicon nitride

Nicola Marzari, Antonio Abate, Ngoc Linh Nguyen

The self-assembly of a single layer of organic molecules on a substrate is a powerful strategy to modify surfaces and interfacial properties. Thiolates, silanes, phosphonates and carboxylates are widely used head-groups to link organic molecules to specifi ...

Royal Society of Chemistry2019

Pressure-induced transformation of CH3NH3PbI3: the role of the noble-gas pressure transmitting media

László Forró, Andrzej Sienkiewicz, Bálint Náfrádi, Endre Horvath, Alla Arakcheeva, Márton Kollár, Gaétan Charles Antoine Giriat, Anastasiia Glushkova

The photovoltaic perovskite, methylammonium lead triiodide [CH3NH3PbI3 (MAPbI(3))], is one of the most efficient materials for solar energy conversion. Various kinds of chemical and physical modifications have been applied to MAPbI(3) towards better unders ...

International Union of Crystallography2019

Photo-physical Properties of Perovskites on Curved Surfaces

Konstantins Mantulnikovs

Organic-inorganic metal halide perovskites (MHPs) have recently attracted increasing attention as highly-efficient light-harvesting materials for photovoltaic applications. The technical ease of solution processing of these materials is one of their major ...

EPFL2019

DNA-BSA interaction, cytotoxicity and molecular docking of mononuclear zinc complexes with reductively cleaved N2S2 Schiff base ligands

Farzaneh Fadaei Tirani, Kurt Schenk

The synthesis of three potentially tetradentate, N2S2 Schiff-base-ligands, containing a disulfide bond, (LSSLThio)-S-Thio(L1), (LSSLBr)-S-Br(L2) and (LSSLDiMeO)-S-DiMeO (L3) are reported. These ligands undergo reductive disulfide bond scission upon reactio ...

ELSEVIER SCIENCE SA2018

Single crystals of superconducting SmFeAsOHx: Structure and properties

László Forró, Alla Arakcheeva, Richard Gaal, Sergiy Katrych, Andrea Pisoni, Ping Huang, Péter Krisztián Matus

We report the synthesis, structure, and superconducting properties of single crystals of SmFeAsOHx. The crystals were grown at high pressure and high temperature using a cubic anvil technique. H-1-NMR studies confirm the presence of H atoms in the samples. ...

Amer Physical Soc2016

In situ synthesis and simulation of polydisperse amphiphilic membranes

Lida Kanari, Julian Charles Shillcock, Liesbeth Maria L Vanherpe

The field of coarse-grained simulations of biopolymers and membranes has grown rapidly in recent years. Industrial groups manufacture and use polymers in fields as diverse as chemicals processing and personal care products, while academic researchers are i ...

Springer India2015