Lecture

Colloidal Synthesis of Nanoparticles

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In course

ChE-430: Nanomaterials for chemical engineering application

This course provides an overview on nanoparticle synthesis and their use in different energy-related applications. The first part of the course is more fundamental and chemistry oriented. The second part is more applied and chemical engineering oriented. T ...

Description

This lecture covers the techniques for the synthesis of nanomaterials, including top-down and bottom-up approaches. It explores the properties and characterization of nanoparticles, focusing on quantum confinement and optical properties. Various methods such as lithography, microcontact printing, and inert gas condensation are discussed, along with their applications in catalysis. The lecture also delves into the role of ligands and surfactants in nanoparticle synthesis, using techniques like Transmission Electron Microscopy and X-Ray Diffraction for characterization.

Instructor

Raffaella Buonsanti

Teaching & PhD PhD Students Riya Gupta, Jennifer Calderon Mora, Coline Boulanger, Moritz Tritschler, Marco Fabbiano, Seyedmohamadjavad Chabok, Hugh Andrew Warkentin Past EPFL PhD Students Chethana Janardhana Gadiyar, Seryio Saris, Valeria Mantella, Seyedehbehnaz Varandili, Pranit Srinivas Iyengar, Yannick Thomas Guntern, Jan Vávra, Laia Castilla Amorós, Valery Okatenko, Ona Segura Lecina, Ludovic Emile Frédy Zaza, Petru Pasquale Albertini Courses Introduction to chemical engineering Laboratory Works

Official source

Ontological neighbourhood

Chemical engineering

Nanotechnology: Topics in nanotechnology

Related concepts (32)

Microcontact printing

Microcontact printing (or μCP) is a form of soft lithography that uses the relief patterns on a master polydimethylsiloxane (PDMS) stamp or Urethane rubber micro stamp to form patterns of self-assembled monolayers (SAMs) of ink on the surface of a substrate through conformal contact as in the case of nanotransfer printing (nTP). Its applications are wide-ranging including microelectronics, surface chemistry and cell biology. Both lithography and stamp printing have been around for centuries.

Scanning transmission electron microscopy

A scanning transmission electron microscope (STEM) is a type of transmission electron microscope (TEM). Pronunciation is [stɛm] or [ɛsti:i:ɛm]. As with a conventional transmission electron microscope (CTEM), images are formed by electrons passing through a sufficiently thin specimen. However, unlike CTEM, in STEM the electron beam is focused to a fine spot (with the typical spot size 0.05 – 0.2 nm) which is then scanned over the sample in a raster illumination system constructed so that the sample is illuminated at each point with the beam parallel to the optical axis.

Cryogenic electron microscopy

Cryogenic electron microscopy (cryo-EM) is a cryomicroscopy technique applied on samples cooled to cryogenic temperatures. For biological specimens, the structure is preserved by embedding in an environment of vitreous ice. An aqueous sample solution is applied to a grid-mesh and plunge-frozen in liquid ethane or a mixture of liquid ethane and propane. While development of the technique began in the 1970s, recent advances in detector technology and software algorithms have allowed for the determination of biomolecular structures at near-atomic resolution.

Electron-beam lithography

Electron-beam lithography (often abbreviated as e-beam lithography, EBL) is the practice of scanning a focused beam of electrons to draw custom shapes on a surface covered with an electron-sensitive film called a resist (exposing). The electron beam changes the solubility of the resist, enabling selective removal of either the exposed or non-exposed regions of the resist by immersing it in a solvent (developing). The purpose, as with photolithography, is to create very small structures in the resist that can subsequently be transferred to the substrate material, often by etching.

Nanomaterial-based catalyst

Nanomaterial-based catalysts are usually heterogeneous catalysts broken up into metal nanoparticles in order to enhance the catalytic process. Metal nanoparticles have high surface area, which can increase catalytic activity. Nanoparticle catalysts can be easily separated and recycled. They are typically used under mild conditions to prevent decomposition of the nanoparticles. Functionalized metal nanoparticles are more stable toward solvents compared to non-functionalized metal nanoparticles.

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