Lecture

EBSD Basics: Applications and Techniques

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In course

MSE-636: Organic semiconductors

Description

This lecture covers the basics of Electron Backscatter Diffraction (EBSD) in Scanning Electron Microscopy (SEM), including orientation measurements, phase identification, and near-surface techniques. It explains how EBSD patterns are obtained, the importance of sample preparation, and the acquisition and indexation of EBSPs. The lecture also discusses the Hough transform for band detection, the influence of accelerating voltage, and the spatial and angular accuracy of EBSD. Furthermore, it explores the applications of EBSD in micro-crystallography, phase identification, and texture analysis, showcasing examples of directional solidification and phase identification in different materials.

Instructor

Frank Nüesch

Teaching & PhD PhD Students Elodie Didier, Ceren Mitmit, João Pedro Ferreira Assunção, Vahid Charkhesht Past EPFL PhD Students Hui Zhang, Simon Johannes Dünki, Yee Song Ko, Lei Wang, Sandra Christina Jenatsch, Nicolas Alexandre Serge Leclaire, Donatas Gesevicius, Surendra Babu Anantharaman, Markus Regnat, Philip Horst Caspari, Patrik Schürch, David Reber, Karen Verena Strassel, Sina Abdolhosseinzadeh, Matthias Diethelm, Francis Owusu, Camilla Arietta Vael-Garn, Yeerlan Adeli, Wei-Hsu Hu, Cansu Zeytun Kara

Official source

Related concepts (32)

Scanning electron microscope

A scanning electron microscope (SEM) is a type of electron microscope that produces images of a sample by scanning the surface with a focused beam of electrons. The electrons interact with atoms in the sample, producing various signals that contain information about the surface topography and composition of the sample. The electron beam is scanned in a raster scan pattern, and the position of the beam is combined with the intensity of the detected signal to produce an image.

Cryogenic electron microscopy

Cryogenic electron microscopy (cryo-EM) is a cryomicroscopy technique applied on samples cooled to cryogenic temperatures. For biological specimens, the structure is preserved by embedding in an environment of vitreous ice. An aqueous sample solution is applied to a grid-mesh and plunge-frozen in liquid ethane or a mixture of liquid ethane and propane. While development of the technique began in the 1970s, recent advances in detector technology and software algorithms have allowed for the determination of biomolecular structures at near-atomic resolution.

Texture (chemistry)

In physical chemistry and materials science, texture is the distribution of crystallographic orientations of a polycrystalline sample (it is also part of the geological fabric). A sample in which these orientations are fully random is said to have no distinct texture. If the crystallographic orientations are not random, but have some preferred orientation, then the sample has a weak, moderate or strong texture. The degree is dependent on the percentage of crystals having the preferred orientation.

Electron microscope

An electron microscope is a microscope that uses a beam of electrons as a source of illumination. They use electron optics that are analogous to the glass lenses of an optical light microscope. As the wavelength of an electron can be up to 100,000 times shorter than that of visible light, electron microscopes have a higher resolution of about 0.1 nm, which compares to about 200 nm for light microscopes.

Electron backscatter diffraction

Electron backscatter diffraction (EBSD) is a scanning electron microscopy (SEM) technique used to study the crystallographic structure of materials. EBSD is carried out in a scanning electron microscope equipped with an EBSD detector comprising at least a phosphorescent screen, a compact lens and a low-light camera. In this configuration, the SEM incident beam hits the tilted sample. As backscattered electrons leave the sample, they interact with the crystal's periodic atomic lattice planes and diffract according to Bragg's law at various scattering angles before reaching the phosphor screen forming Kikuchi patterns (EBSPs).

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