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Microscopic Mechanical Properties and Physicochemical Changes of Cement Paste Exposed to Elevated Temperatures and Subsequent Rehydration

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1H–19F cross-polarization magic angle spinning dynamic nuclear polarization NMR investigation of advanced pharmaceutical formulations

David Lyndon Emsley

A new 3.2 mm 1H–19F–X magic angle spinning dynamic nuclear polarization NMR (MAS DNP-NMR) probe was developed with a unique coil design with separate radiofrequency channels for 1H excitation and 13C or 19F detection to enable acquisition of 1H–19F cross-p ...

Academic Press Inc - Elsevier Science2025

Rosette Spectroscopic Imaging for Whole-Brain Slab Metabolite Mapping at 7T: Acceleration Potential and Reproducibility

Lijing Xin, Mark Stephan Widmaier, Ying Xiao, Zhiwei Huang, André Döring

Whole-brain proton magnetic resonance spectroscopic imaging (H-1-MRSI) is a non-invasive technique for assessing neurochemical distribution in the brain, offering valuable insights into brain functions and neural diseases. It greatly benefits from the impr ...

Wiley2025

Pulsed Magnetophononics in Gapped Quantum Magnets

Baptiste Paul Eloi Demazure

One route to the control of quantum magnetism at ultrafast timescales is magnetophononics, the modulation of magnetic interactions by coherently driven lattice excitations. Theoretical studies of a gapped quantum magnet subject to continuous, single-freque ...

AMER PHYSICAL SOC2025

Investigating the ball-milled calcined coal gangue on the hydration of limestone blended cement

Lei Xu

Calcined coal gangue (CCG) exhibits promising application potential in limestone-cement binary binders. However, the activity of CCG would possibly be weakened due to the particle agglomeration after calcination. In the present research, we tried to overco ...

2025

Magic Angle Spinning Solid-State 13C Photochemically Induced Dynamic Nuclear Polarization by a Synthetic Donor-Chromophore-Acceptor System at 9.4 T

David Lyndon Emsley, Michael Allan Hope, Federico De Biasi, Máté Visegrádi

Solid-state photochemically induced dynamic nuclear polarization (photo-CIDNP) is a nuclear magnetic resonance spectroscopy technique in which nuclear spin hyperpolarization is generated upon optical irradiation of an appropriate donor-acceptor system. Unt ...

Amer Chemical Soc2024

Solid Effect Dynamic Nuclear Polarization Enhancement of >500 at 9.4 T

David Lyndon Emsley, Yu Rao, Amrit Venkatesh, Ran Wei

Efficient polarizing agents for dynamic nuclear polarization (DNP) enhanced magic angle spinning (MAS) NMR spectroscopy is of high current interest due the potential to significantly boost NMR sensitivity. While most efforts have centered on cross-effect ( ...

American Chemical Society (ACS)2024

Structural study of nickelate based heterostructures

Duncan Thomas Lindsay Alexander, Bernat Mundet, Chih-Ying Hsu

Heterostructures consisting of SmNiO3 and NdNiO3 alternating layers with additional LaAlO3 spacer layers were grown and fully characterized by means of x-ray diffraction, atomic force microscopy, and scanning transmission electron microscopy. A change in t ...

Aip Publishing2024

Overhauser enhanced liquid state nuclear magnetic resonance spectroscopy in one and two dimensions

Marcel Levien

Nuclear magnetic resonance (NMR) is fundamental in the natural sciences, from chemical analysis and structural biology, to medicine and physics. Despite its enormous achievements, one of its most severe limitations is the low sensitivity, which arises from ...

NATURE PORTFOLIO2024

Partial crystallization in Pd-BMG systems: From understanding structure towards influencing functionality through temperature-time series

Roland Logé

Small quantities of crystalline domains created in an amorphous matrix are seen as an active driver for enhanced properties in bulk metallic glasses (BMGs). We investigated partial crystallization and phase transformations through a series of isotherms at ...

2024

Melting Curve of Black Phosphorus: Evidence for a Solid-Liquid-Liquid Triple Point

Tomasz Poreba

Black phosphorus (bP) is a crystalline material that can be seen as an ordered stacking of two-dimensional layers, which results in outstanding anisotropic physical properties. The knowledge of its pressure (P)-temperature (T) phase diagram, and in particu ...

AMER CHEMICAL SOC2024

Disused Concrete, Digital Acupuncture and Reuse

Corentin Jean Dominique Fivet, Maléna Bastien Masse, Stefana Parascho, Maxence Grangeot

Crushing concrete liberated from demolished buildings to provide recycled aggregate is argued to be a sustainable way of reducing material extraction. Yet, in these high‐energy processes, large amounts of new cement is often used, negating this as a low‐ca ...

Wiley2024

Overcoming the probing-depth dilemma in spectroscopic analyses of batteries with muon-induced X-ray emission (MIXE)

Corsin Battaglia

Battery research often encounters the challenge of determining chemical information, such as composition and elemental oxidation states, of a layer buried within a cell stack in a non-destructive manner. Spectroscopic techniques based on X-ray emission or ...

Royal Society of Chemistry2024

Kinetics of Al uptake in synthetic calcium silicate hydrate (C-S-H)

Karen Scrivener

The effect of equilibration time on the composition, structure and solubility of calcium aluminate silicate hydrate (C-A-S-H) was investigated in 0.5 M NaOH solutions at Al/Si = 0.1. Longer equilibration time led to longer silica chains, to less Na and, to ...

Pergamon-Elsevier Science Ltd2023

The Beneficial Effect of Oral Cr Supplementation in an Early Childhood Rat Model of Chronic Hepatic Encephalopathy: In Vivo Longitudinal 1H and 31P Magnetic Resonance Spectroscopy Study

Cristina Ramona Cudalbu Moldovan, Dunja Simicic, Katarzyna Pierzchala, Stefanita-Octavian Mitrea

Lippincott Williams & Wilkins2023

Multi-sample/multi-nucleus parallel polarization and monitoring enabled by a fluid path technology compatible cryogenic probe for dissolution dynamic nuclear polarization

Andrea Capozzi, Jean-Noël Hyacinthe, Thanh Phong Kevin Lê

Low throughput is one of dissolution Dynamic Nuclear Polarization (dDNP) main shortcomings. Especially for clinical and preclinical applications, where direct 13C nuclei polarization is usually pursued, it takes hours to generate one single hyperpolarized ...

Nature Research2023

Effect of Mo addition on the mechanical and tribological properties of magnetron sputtered TiN films

Sami Rtimi

Ternary-based titanium nitride (TiN) thin films have drawn attention toward rational applications due to their wear resistance, high hardness, and corrosion resistance. The influence of Mo content on the structural, tribo-logical, and mechanical properties ...

ELSEVIER SCIENCE SA2023

Resonators with tailored optical path by cascaded-mode conversions

Ileana-Cristina Benea-Chelmus

Optical resonators enable the generation, manipulation, and storage of electromagnetic waves. The physics underlying their operation is determined by the interference of electromagnetic waves, giving rise to the resonance spectrum. This mechanism causes th ...

Nature Portfolio2023

Insights on chemical and physical chloride binding in blended cement pastes

Karen Scrivener, Fabien Jacques Michel Georget, William Wilson

This study investigates chloride binding in blended cement pastes exposed to 0.5 M NaCl solutions (with and without pH adjustment) using X-ray diffraction and energy-dispersive X-ray spectroscopy image analysis (edxia). The aim is to better understand the ...

Pergamon-Elsevier Science Ltd2022

Hyperpolarized (1-13C)Alaninamide Is a Multifunctional In Vivo Sensor of Aminopeptidase N Activity, pH, and CO2

Rolf Gruetter, Hikari Ananda Infinity Yoshihara, Daniel Ortiz Trujillo, Alice Radaelli

Spin hyperpolarization enables real-time metabolic imaging of carbon-13-labeled substrates. While hyperpolarized L- (1-13C)alaninamide is a probe of the cell-surface tumor marker aminopeptidase-N (APN, CD13), its activity in vivo has not been described. Sc ...

AMER CHEMICAL SOC2022

An investigation on reorientation and textural evolution in a martensitic NiTi rolled sheet using EBSD

Roland Logé, Cyril Cayron, Junfeng Xiao

Variant reorientation is a ubiquitous phenomenon in shape memory alloys and has a great influence on their texture and mechanical response. In the present study, a martensitic NiTi rolled sheet is investigated by the electron backscattering diffraction (EB ...

PERGAMON-ELSEVIER SCIENCE LTD2022