Publication

A large-scale low-cost access to the lithium 2,2,6,6-tetramethylpiperidide precursor

Manfred Schlosser, Fabrice Cottet, Frédéric Leroux
2005
Journal Articles

Abstract

Wolff-Kishner-Huang redn. of the cheap 2,2,6,6-tetramethyl-4-piperidinone provides the expensive 2,2,6,6-tetramethylpiperidine, the precursor to lithium 2,2,6,6-tetramethylpiperidide, in high yield. As specified in the detailed protocol, the reaction can be conveniently carried out on a >10 mol lab. scale. [on SciFinder (R)]

Official source

https://infoscience.epfl.ch/entities/publication/7c6a5667-c5ee-4f1c-bb5a-03c38d7d9f8c

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